OSU Microscopy Facility
PUBLICATIONS
2025
- Caron C, McCullagh EA, Bertolin G. Sex-specific loss of mitochondrial membrane integrity
in the auditory brainstem of a mouse model of Fragile X Syndrome. Open Biol. 15, 240384 (2025). https://doi.org/10.1098/rsob.240384
- Phadindra Wagle, Punya Mainali, Saraswati Shrestha, Ujjal Lamichhane, Derek Meyers,
and D. N. McIlroy, J. Appl. Phys.137, 065302 (2025). https://doi.org/10.1063/5.0228821
- Bret A. Marckx, Hunter Maclennan, and Ömer Özgür Capraz, Probing Electrochemical
Strain Generation in Vanadium Oxide Cathodes during Cycling of Aqueous Zinc-Ion Batteries
via Imaging Technique. Chemical & Biomedical Imaging special issue “Imaging in Energy
Science” (2025). https://doi.org/10.1021/cbmi.5c00003
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Pratt, Carrie J., Emma E. England, Julia M. Vinzelj, Noha H. Youssef, and Mostafa S. Elshahed. Anaeromyces corallioides, sp. nov., a new anaerobic gut fungus from the faeces of cattle. International Journal of Systematic and Evolutionary Microbiology 75, 006719 (2025). https://doi.org/10.1099/ijsem.0.006719
2024 - Zhukov, A. and Popov, V., Eukaryotic cell membranes: structure, composition, research
methods and computational modelling. International Journal of Molecular Sciences,
24(13), 11226 (2024). https://doi.org/10.3389/fmicb.2023.1339303
- Julius de Rojas, Del Atkinson and Adekunle O Adeyeye, Tailoring magnon modes by extending
square, kagome, and trigonal spin ice lattices vertically via interlayer coupling
of trilayer nanomagnets, J. Phys.: Condens. Matter 36 415805 (2024). https://doi.org/1088/1361-648X/ad5d3f
- U. Lamichhane, B. Sankhi, N. Kundu, G. Fabbris, Y. Choi, D. Haskel, J. L. McChesney,
Yue Cao, J. Li, V. Bisogni, M. F. Borunda, and D. Meyers, Electronic reconstruction
in confined SrRuO3 monolayers, Phys. Rev. B, 110, 235104 (2024). https://doi.org/10.1103/PhysRevB.110.235104
- Songpei Xie, Amir Erfani, Saeed Manouchehri, Joshua Ramsey, Clint Aichele, Aerosolization
of poly(sulfobetaine) microparticles that encapsulate therapeutic antibodies, Biomaterials
Advances 160, 213839 (2024). https://doi.org/1016/j.bioadv.2024.213839
- Sharma S, Khatri N, Puri S, Adhikari M, Wagle P, McIlroy DN, Kalkan AK, Vasquez Y*. Iron Phosphide Nanobundles for Efficient Electrochemical Hydrogen Evolution Reaction
in Acidic and Basic Media. ACS Applied Materials & Interfaces, 16(45), 61858-61867 (2024). https://doi.org/10.1021/acsami.4c09660
- McIlroy, D. N., Jean-Jacques Gaumet, Philippe Pierrat, Pierre Magri, Pascal Franchetti,
Chris Hocevar, Brenden H. Martin, John O’hara, and Nathan P. Dice. "Surface Plasmon
Polariton Scattering, Light Emission, and Diffraction Phenomena of Highly Contoured
Gold Mesostructures." Plasmonics 1-14 (2024). https://doi.org/10.1007/s11468-024-02647-0
- Xiong, Fengyang, Yulun Wang, Jim Puckette, Michael Grammer, Gabriel Awejori, and Mileva
Radonjic. "Geochemical and Microstructural Characterization of Shale Rock: A Workflow
for Site Evaluation for Energy–Fluids Storage." Energy & Fuels 38, 20875-20891 (2024).
https://doi.org/10.1021/acs.energyfuels.4c03197
- Awejori, Gabriel A., Wenming Dong, Christine Doughty, Nicolas Spycher, and Mileva
Radonjic. "Mineral and fluid transformation of hydraulically fractured shale: case
study of Caney Shale in Southern Oklahoma." Geomechanics and Geophysics for Geo-Energy
and Geo-Resources 10, 128 (2024). https://doi.org/10.1007/s40948-024-00835-0
- Awejori, Gabriel A., Wenming Dong, Christine Doughty, Nicolas Spycher, and Mileva
"Mineralogy and reactive fluid chemistry evolution of hydraulically fractured Caney
shale of Southern Oklahoma." Gas Science and Engineering 131, 205458 (2024). https://doi.org/10.1016/j.jgsce.2024.205458
2023 - Adhikari M, Sharma S, Echeverria E, McIlroy DN, Vasquez Y. Formation of Iron Phosphide
Nanobundles from an Iron Oxyhydroxide Precursor. ACS Nanoscience Au, 3(6), 491-499 (2023). https://doi.org/10.1021/acsami.4c09660
- Addanki Tirumala, Ravi Teja, Nishan Khatri, Sundaram Bhardwaj Ramakrishnan, Farshid
Mohammadparast, Mohd Tauhid Khan, Susheng Tan, Phadindra Wagle, Sharad Puri, David
N. McIlroy, Ali Kaan Kalkan, Marimuthu Andiappan, "Tuning Catalytic Activity and Selectivity
in Photocatalysis on Mie-Resonant Cuprous Oxide Particles: Distinguishing Electromagnetic
Field Enhancement Effect from the Heating Effect." ACS Sustainable Chemistry & Engineering
11, no. 44 15931-15940 (2023). https://doi.org/10.1021/acssuschemeng.3c04328
- Mainali, Punya, Phadindra Wagle, Nishan Khatri, Chasen McPherson, Kaan Kalkan, and
D. N. McIlroy. "Humidity induced resistive switching and negative differential resistance
in α-Fe2O3 porous thin films." Sensors and Actuators A: Physical 362, 114631 (2023).
https://doi.org/10.1016/j.sna.2023.114631
- Dice, Nathan P., Aaron J. Austin, Phadindra Wagle, Emrah Turgut, and D. N. McIlroy.
"Understanding gold mesopyramid formation on silicon and strategies for creating patterns
of them." Materials Science and Engineering: B 297, 116759 (2023). https://doi.org/10.1016/j.sna.2023.11463
- Ronte, Anil, Phadindra Wagle, Ghader Mahmodi, Mounika Chevula, Shailesh Dangwal, Mohammad
Reza Saeb, Jong Suk Lee, David N. Mcllroy, and Seok-Jhin Kim. "High-flux ZIF-8 membranes
on ZnO-coated supports for propane/propylene separation."Energy & Fuels 37, no. 12, 8456-8464 (2023). https://doi.org/10.1021/acs.energyfuels.3c00212
- Sankhi, Babu R., Elena M. Echeverria, Soumya Mandal, Muhammet Annaorazov, Ritesh Sachan,
David N. Mcllroy, Derek Meyers, and Emrah Turgut. "Engineering Pt/Co/AlO x heterostructures
to enhance the dzyaloshinskii–Moriya interaction." Journal of Physics: Condensed Matter
35, 145802 (2023). https://doi.org/10.1088/1361-648X/acba73
- Mainali, Punya, Phadindra Wagle, Chasen McPherson, and David N. McIlroy. "The Impact
of Trap-Assisted Tunneling and Poole–Frenkel Emission on Synaptic Potentiation in
an α-Fe2O3/p-Si Memristive Device." Sci 5, 3 (2023). https://doi.org/10.3390/sci5010003
- Katende, Allan, Jonny Rutqvist, Cody Massion, and Mileva Radonjic. "Experimental flow-through
a single fracture with monolayer proppant at reservoir conditions: A case study on
Caney Shale, Southwest Oklahoma, USA." Energy 273, 127181 (2023). https://doi.org/10.1016/j.energy.2023.127181
- Katende, Allan, Connor Allen, Jonny Rutqvist, Seiji Nakagawa, and Mileva Radonjic.
"Experimental and numerical investigation of proppant embedment and conductivity reduction
within a fracture in the Caney Shale, Southern Oklahoma, USA." Fuel 341, 127571 (2023).
https://doi.org/10.1016/j.fuel.2023.127571
- Benge, Margaret, Allan Katende, Jonny Rutqvist, Mileva Radonjic, and Andrew Bunger.
"Creep properties of shale and predicted impact on proppant embedment for the Caney
Shale, Oklahoma." Rock Mechanics and Rock Engineering 56, 5903-5921 (2023). https://doi.org/10.1007/s00603-023-03362-8
- Massion, Cody, Vamsi SK Vissa, Yunxing Lu, Dustin Crandall, Andrew Bunger, and Mileva
Radonjic. "Geomimicry-inspired micro-nano concrete as subsurface hydraulic barrier
materials: learning from shale rocks as best geological seals." In REWAS 2022: Energy
Technologies and CO2 Management (Volume II), pp. 129-138. Cham: Springer International
Publishing, (2022). https://doi.org/10.1007/978-3-030-92559-8_13
- Gregory, Darrell, Sisi Yang, Cody Massion, Matthew Mecklenburg, Indu Aravind, Mileva
Radonjic, Stephen Cronin, and Ömer Özgür Çapraz. "Utilizing nanoscale particulate
matter from the combustion of diesel fuels as a carbonaceous anode electrode for Li-ion
batteries." Resources, Conservation and Recycling 177, 105972 (2024). https://doi.org/10.1016/j.geothermics.2023.102812
- Carpenter, Kristen Courtney, Loic Bethel Dje, Mercy Achang, and Mileva Radonjic. "Comparative
laboratory study of the geochemical reactivity of the marcellus shale: rock–fluid
interaction of drilled core samples vs. outcrop specimens." Water 15, 1940 (2023).
https://doi.org/10.3390/w15101940
- Vissa, Sai Vamsi Krishna, Cody Massion, Yunxing Lu, Andrew Bunger, and Mileva Radonjic.
"Zeolite-Enhanced Portland Cement: Solution for Durable Wellbore-Sealing Materials."
Materials 16, 30 (2022). https://doi.org/10.3390/ma16010030
- Jupudi, Havila, Cody Massion, and Mileva Radonjic. "The impact of graphene nanoplatelets
(GNPs) on the hydration mechanism of alite (C3S) in Class-H wellbore cement with focus
on microstructural properties." In TMS Annual Meeting & Exhibition, pp. 1322-1330.
Cham: Springer Nature Switzerland, (2023). https://doi.org/10.1007/978-3-031-22524-6_128
- Awejori, Gabriel, Havila Jupudi, Cody Massion, and Mileva Radonjic. "Study on Advanced
Cementing Practices Using Inert Graphene Nanoplatelets and Hydraulic Fracturing Fluids
for Wellbore Integrity and Sustainability." In TMS Annual Meeting & Exhibition, pp.
1225-1236. Cham: Springer Nature Switzerland, (2023). https://doi.org/10.1007/978-3-031-22524-6_117
2022 - McCullagh EA et al. Auditory brainstem development of naked mole-rats (Heterocephalus
glaber), Proc. R. Soc. B 289: 20220878 (2022). https://doi.org/10.1098/rspb.2022.0878
- Gregory, Darrell, Sisi Yang, Cody Massion, Matthew Mecklenburg, Indu Aravind, Mileva
Radonjic, Stephen Cronin, and Ömer Özgür Çapraz, Utilizing nanoscale particulate matter
from the combustion of diesel fuels as a carbonaceous anode electrode for Li-ion batteries.
Resources, Conservation and Recycling 177, 105972 (2022). https://doi.org/10.1016/j.resconrec.2021.105972
- Austin, Aaron J., Nathan P. Dice, Elena Echeverria, Ashish Kumar Gupta, Jonathan Risner,
Halle C. Helfrich, Ritesh Sachan, and David N. McIlroy. "Magnesium Sublimation for
Growing Thin Films and Conformal Coatings on 1D Nanostructures." Nanomanufacturing
2, 186-193 (2022). https://doi.org/10.3390/nanomanufacturing2040013
- Ronte, Anil, Shailesh Dangwal, Han Lin, Phadindra Wagle, Elena Echeverria, Jong Suk
Lee, Jiahua Zhu, David N. McIlroy, and Seok-Jhin Kim. "Modification of ZIF-8 membranes
by atomic layer deposition for high propylene/propane selectivity." Microporous and
Mesoporous Materials 343, 112173 (2022). https://doi.org/10.1016/j.micromeso.2022.112173
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Mandal, Soumya, Ashish Kumar Gupta, Elena Echeverria, David N. McIlroy, Jonathan D. Poplawsky, and Ritesh Sachan. "Laser-assisted nanofabrication of multielement complex oxide core–shell nanoparticles." Materials & Design 220, 110882 (2022). https://doi.org/10.1016/j.matdes.2022.110882
- Massion, Cody, Yunxing Lu, Dustin Crandall, Andrew Bunger, and Mileva Radonjic. "Graphene
nanoplatelets reinforced cement as a solution to leaky wellbores reinforcing weak
points in hydrated Portland cement with graphene nanoparticles improves mechanical
and chemical durability of wellbore cements." Cement and Concrete Composites 133,
104726 (2022). https://doi.org/10.1016/j.cemconcomp.2022.104726
- Adua Awejori, Gabriel, Christine Doughty, Fengyang Xiong, Thomas Paronish, Nicholas
Spycher, and Mileva Radonjic. "Integrated experimental and modeling study of geochemical
reactions of simple fracturing fluids with Caney Shale." Energy & Fuels 36, 10064-10081
(2022). https://doi.org/10.1021/acs.energyfuels.2c01739
2021 - Jain V, Shelby T, Patel T, Mekhedov E, Petersen JD, Zimmerberg J, Ranaweera A, Wellky
DP, Dandawate P, Anant S, Sulthana S, Vasquez Y, Banerjee T, Santra S. A Bimodal Nanosensor
for Probing Influenza Fusion Protein Activity Using Magnetic Relaxation. ACS Sensors,
6 (5), 1899-1909 (2021) https://doi.org/10.1021/acssensors.1c00253
- Dice, Nathan, Aaron J. Austin, and David McIlroy. "Exploiting eutectic formation and
phase separation to produce plasmonic metamaterials." Journal of Applied Physics 130,
12 (2021). https://doi.org/10.1063/5.0060713
- Mainali, Punya, Lyndon D. Bastatas, Elena Echeverria, Phadindra Wagle, Prasanna Sankaran, and D. N. Mcilroy. "Addressing crosstalk in crossbar memory arrays with a resistive switching ZnO homojunction diode." Journal of Applied Physics 129, no. 20 (2021). https://doi.org/10.1063/5.0050564
- Katende, Allan, Lisa O’Connell, Ashley Rich, Jonny Rutqvist, and Mileva Radonjic.
"A comprehensive review of proppant embedment in shale reservoirs: Experimentation,
modeling and future prospects." Journal of Natural Gas Science and Engineering 95,
104143 (2021). https://doi.org/10.1016/j.jngse.2021.104143
- Katende, Allan, Jonny Rutqvist, Margaret Benge, Abbas Seyedolali, Andrew Bunger, James
O. Puckette, Andy Rhin, and Mileva Radonjic. "Convergence of micro-geochemistry and
micro-geomechanics towards understanding proppant shale rock interaction: A Caney
shale case study in southern Oklahoma, USA." Journal of Natural Gas Science and Engineering
96, 104296 (2021). https://doi.org/10.1016/j.jngse.2021.104296
- Achang, Mercy, and Mileva Radonjic. "Adding olivine micro particles to Portland cement
based wellbore cement slurry as a sacrificial material: A quest for the solution in
mitigating corrosion of wellbore cement." Cement and Concrete Composites 121, 104078
(2021). https://doi.org/10.1016/j.cemconcomp.2021.104078
- Wang, Yulun, Guofan Luo, Mercy Achang, Julie Cains, Conn Wethington, Allan Katende,
G. Michael Grammer et al. "Multiscale characterization of the Caney Shale—an emerging
play in Oklahoma." Midcontinent Geoscience 2, 33-53 (2021). https://doi.org/10.17161/mg.v2i.15911
2020 - Adhikari M, Echeverria E, Risica G, McIlroy DN, Nippe M, Vasquez Y. Synthesis of Magnetite
Nanorods from the Reduction of Iron Oxy-Hydroxide with Hydrazine. ACS Omega, 5 (35),
22440-22448 (2020). https://doi.org/10.1021/acsomega.0c02928
- Adhikari M, Singh A, Echeverria E, McIlroy DN, Vasquez Y*. Iron Pyrite Nanocrystals:
A Potential Catalyst for Selective Transfer Hydrogenation of Functionalized Nitroarenes.
ACS Omega, 5 (23), 14104-14110 (2020). https://doi.org/10.1021/acsomega.0c01637
- Deshani Fernando, Shoukath Sulthana, and Yolanda Vasquez, Cellular Uptake and Cytotoxicity
of Varying Aspect Ratios of Gold Nanorods in HeLa Cells, ACS Appl. Bio Mater. 3, 1374−1384
(2020). https://pubs.acs.org/doi/10.1021/acsabm.9b00986
- Austin, Aaron J., Elena Echeverria, Phadindra Wagle, Punya Mainali, Derek Meyers,
Ashish Kumar Gupta, Ritesh Sachan, S. Prassana, and David N. McIlroy. "High-temperature
atomic layer deposition of GaN on 1D nanostructures." Nanomaterials 10, 2434 (2020).
https://doi.org/10.3390/nano10122434
- Mahmodi, Ghader, Shailesh Dangwal, Payam Zarrintaj, Mengfan Zhu, Yu Mao, David N.
Mcllroy, Mohammad Reza Saeb, Vahid Vatanpour, Joshua D. Ramsey, and Seok-Jhin Kim.
"NaA zeolite-coated meshes with tunable hydrophilicity for oil-water separation."
Separation and Purification Technology 240, 116630 (2020). https://doi.org/10.1016/j.seppur.2020.116630
2019 - Sourabh Biswasa, S. Habib Alavia, Bhishma Sedaib, Frank D. Blumb, Sandip P. Harimkar,
Effect of ultrasonic vibration-assisted laser surface melting and texturing of Ti-6Al-4V
ELI alloy on surface properties, Journal of Materials Science & Technology 35, 295–302,
(2019). https://doi.org/10.1016/j.jmst.2018.09.057
- Hasani G. Jayasinghe, Sundararajan V. Madihally, and Yolanda Vasquez, Formation of
Stem Cell Aggregates and Their Differentiation on Surface-Patterned Hydrogels Based
on Poly(2-hydroxyethyl Methacrylate), ACS Appl. Bio Mater. 2, 4911−4921 (2019). https://pubs.acs.org/doi/abs/10.1021/acsabm.9b00661
- Dangwal, Shailesh, Ruochen Liu, Lyndon D. Bastatas, Elena Echeverria, Chengqian Huang,
Yu Mao, David N. Mcllroy, Sangil Han, and Seok-Jhin Kim. "ZnO microfiltration membranes
for desalination by a vacuum flow-through evaporation method." Membranes 9, 156 (2019).
https://doi.org/10.3390/membranes9120156
- Wojcik, Peter M., Negar Rajabi, Haoyu Zhu, David Estrada, Paul H. Davis, Twinkle Pandhi,
I. Francis Cheng, and David N. McIlroy. "Utilizing a Single Silica Nanospring as an
Insulating Support to Characterize the Electrical Transport and Morphology of Nanocrystalline
Graphite." Materials 12, 3794 (2019). https://doi.org/10.3390/ma12223794
- Walgama, Charuksha, Anuruddha Pathiranage, Mayowa Akinwale, Roberto Montealegre, Jinesh
Niroula, Elena Echeverria, David N. McIlroy, Tres A. Harriman, Don A. Lucca, and Sadagopan
Krishnan. "Buckypaper–Bilirubin Oxidase Biointerface for Electrocatalytic Applications:
Buckypaper Thickness." ACS Applied Bio Materials 2, 2229-2236 (2019). https://doi.org/10.1021/acsabm.9b00189
- Bastatas, Lyndon D., Phadindra Wagle, Elena Echeverria, Aaron J. Austin, and David
N. McIlroy. "The Effect of UV Illumination on the room temperature detection of vaporized
ammonium nitrate by a ZnO coated nanospring-based sensor." Materials 12, 302 (2019).
https://doi.org/10.3390/ma12020302
- Echeverria, Elena, Amrit Kaphle, Aaron Austin, Lyndon Bastatas, Parameswar Hari, and
David Mcllroy. "Evolution of the stoichiometry and electronic structure of cobalt
oxide in thermally treated Co-Doped ZnO nanorods for solar cells." ACS Applied Nano
Materials 2, 4113-4120 (2019). https://doi.org/10.1021/acsanm.9b00574
- Bastatas, Lyndon D., Phadindra Wagle, Elena Echeverria, Jason D. Slinker, and David
N. McIlroy. "Electrical characterization of ZnO-coated nanospring ensemble by impedance
spectroscopy: Probing the effect of thermal annealing." Nanotechnology 30, 234006
(2019). https://doi.org/10.1088/1361-6528/ab087c
2018 - Yi-Wei Wang, Ruiqing Shen, Qingsheng Wang, and Yolanda Vasquez, ZnO Microstructures
as Flame-Retardant Coatings on Cotton Fabrics, ACS Omega 3, 6330−633 (2018). https://pubs.acs.org/doi/abs/10.1021/acsomega.8b00371
- Hasani G. Jayasinghe, Christian J. Tormos, Mughees Khan, Sundar Madihally, Yolanda
Vasquez, A Soft Lithography Method to Generate Arrays of Microstructures onto Hydrogel
Surfaces, J. Polym. Sci., Part B: Polym. Phys. 56, 1144–1157 (2018). https://doi.org/10.1002/polb.24634
- Iyer JK, Dickey A, Rouhani P, Kaul A, Govindaraju N, Singh RN, et al. Nanodiamonds
facilitate killing of intracellular uropathogenic E. coli in an in vitro model of
urinary tract infection pathogenesis. PLoS ONE 13(1): e0191020 (2018). https://doi.org/10.1371/journal.pone.0191020
- Liu, Ruochen, Seth Young, Shailesh Dangwal, Imran Shaik, Elena Echeverria, David McIlroy,
Clint Aichele, and Seok-Jhin Kim. "Boron substituted MFI-type zeolite-coated mesh
for oil-water separation." Colloids and Surfaces A: Physicochemical and Engineering
Aspects 550, 108-114 (2018). https://doi.org/10.1016/j.colsurfa.2018.04.038
- Rajabi, Negar, Peter M. Wojcik, Lokendra R. Khanal, You Qiang, and David N. McIlroy.
"A comparison of the morphological and electrical properties of sol-gel dip coating
and atomic layer deposition of ZnO on 3D nanospring mats." Materials Research Express
6, 035902 (2018). https://doi.org/10.1088/2053-1591/aaf440
- Nwamba, O. Charles, Elena Echeverria, David N. McIlroy, Aaron Austin, Jean’ne M. Shreeve,
and D. Eric Aston. "Thermal modification of graphite for fast electron transport and
increased capacitance." ACS Applied Nano Materials 2, 228-240 (2018). https://doi.org/10.1021/acsanm.8b01887
- Bastatas, Lyndon D., Elena Echeverria-Mora, Phadindra Wagle, Punya Mainali, Aaron
Austin, and David N. McIlroy. "Emergent electrical properties of ensembles of 1D nanostructures
and their impact on room temperature electrical sensing of ammonium nitrate vapor."
ACS sensors 3, 2367-2374 (2018). https://doi.org/10.1021/acssensors.8b00746
2016 - Jessica M. Morrison, Mostafa S. Elshahed & Noha H. Youssef, Defined enzyme cocktail
from the anaerobic fungus Orpinomyces sp. strain C1A effectively releases sugars from
pretreated corn stover and switchgrass, Scientific Reports 6, 29217 (2016). https://doi.org/1038/srep29217
- Fernando D, Nigro A.E.T, Dyer D.I, Alia M.S., Pivovar S.B., Vasquez Y. Synthesis and
catalytic activity of the metastable phase of gold phosphide. Journal of Solid State Chemistry, 242,182-192 (2016). https://doi.org/10.1016/j.jssc.2016.07.009
2015 - Fernando D., Khan M., Vasquez Y. Control of the crystalline phase and morphology of
CdS deposited on microstructured surfaces. Materials Science in Semiconductor Processing,
30, 174-180 (2015).
https://doi.org/10.1016/j.mssp.2014.10.002
2014 - Athauda J.T., Bandarage U. S. K. M., Vasquez Y. Integration of ZnO/ZnS nanostructured
materials into a cotton fabric. RSC Advances., 4, 61327-6133 (2014). https://doi.org/10.1039/C4RA12074D
2012 - Martha E. Hilburn, Befrika S. Murdianti, Randall D. Maples, Jason S. Williams, Joshua
T. Damron, Satish I. Kuriyavar, Kevin D. Ausman, Synthesizing aqueous fullerene colloidal
suspensions by new solvent-exchange methods Colloids and Surfaces A: Physicochem. Eng. Aspects 401 48–53 (2012). https://doi.org/10.1016/j.colsurfa.2012.03.010